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Grob test mixture

Method:
Matrix
Application-No.:
GC
211250

Substances: decane-n; octanol-1; undecane-n; dimethylphenol-2,6; dimethylaniline-2,6; methyl decanoate; methyl undecanoate; dicyclohexylamine; methyl dodecanoate
Column: OPTIMA® 5, 1.0 μm film, 50 m x 0.25 mm ID
Phase: OPTIMA 5
MN catalog number:
Sample pretreatment:
Conditions: Injection: 1 μl, split 1: 40, 280 °C
Carrier gas: 1.5 bar H2
Temperature: 80 °C -> 280 °C (10 min), 8 °C/min
Detection
Subsequent analysis:
FID, 280 °C

Author(-s): GC department
Source: MACHEREY-NAGEL

Keywords: Grob test mixture
Chromatogram:


Legend: 1. n-Decane
2. 1-Octanol
3. n-Undecane
4. 2,6-Dimethylphenol
5. 2,6-Dimethylaniline
6. Methyl decanoate
7. Methyl undecanoate
8. Dicyclohexylamine
9. Methyl dodecanoate



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