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| PAH and PCB from Blood, Serum and Plasma |
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Method:
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Matrix
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Application-No.:
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SPE
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blood
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301350
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| Substances: |
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PAHs; PCBs
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| Column: |
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CHROMABOND® C18 ec, 1 mL, 100 mg |
| Phase: |
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CHROMABOND® C18 ec |
| REF number: |
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730011 |
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| Sample pretreatment: |
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Mix 1 mL sample with 1 mL water / n-propanol (85:15, v/v) and centrifuge for
10 min at 3000 U/min |
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| Conditions: |
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Column conditioning:
2 column volumes methanol, then 2 column volumes dist. water / n-propanol
(85:15, v/v)
Sample application:
Slowly force or aspirate the sample through the column
Column washing:
2 x 500 μL dist. water / n-propanol (85:15, v/v), dry in stream of air or nitrogen
Elution:
2 x 250 μL dichloromethane |
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| Author(-s): |
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SPE department
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| Source: |
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MACHEREY-NAGEL |
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| Keywords: |
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PAHs, PCBs, blood, serum, plasma
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| www.mn-net.com |
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Concerning questions to literature applications please contact the cited author/s. Chemicals mentioned in applications are not manufactured or sold by MACHEREY-NAGEL. Applications mentioned in MACHEREY-NAGEL literature or databases are provided for informational purposes only. MACHEREY-NAGEL does not warrant that all applications have been tested in MACHEREY-NAGEL laboratories using MACHEREY-NAGEL products.
MACHEREY-NAGEL does not warrant the correctness of the applications. |
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