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Analysis of PAH on Optima® 5 MS

Method:
Matrix
Application-No.:
GC

211160




Substances:
Naphthalene; Acenaphthylene; Acenaphthene; Fluorene; Phenanthrene; Anthracene;
Fluoranthene; Pyrene; Benz[a]anthracene; Chrysene; Benzo[b]fluoranthene;
Benzo[k]fluoranthene; Benzo[a]pyrene; Indeno[1,2,3-cd]pyrene; Dibenz[ah]anthracene;
Benzo[ghi]perylene
Column:
OPTIMA® 5 MS, length 30 m, ID 0.25 mm, film thickness 0.25 μm
Phase:
OPTIMA® 5 MS
REF number:
726220.30



Sample:
20 µg/mL in toluene



Conditions:
Injection volume: 0.1 µL, 280 °C
Split: 13 mL/min
Carrier gas: He, 0.9 bar
Temperature: 100 °C -> 300 °C, 7 °C/min (15 min)



Detection:
MSD HP 5971, 280 °C



Author(-s):
GC department
Source:
MACHEREY-NAGEL



Keywords:
PAHs; MS






Chromatogram:





Legend:
5.33   -   Naphthalene
9.62   -   Acenaphthylene
10.22 -   Acenaphthene
11.89 -   Fluorene
15.15 -   Phenanthrene
15.31 -   Anthracene
19.38 -   Fluoranthene
20.15 -   Pyrene
24.48 -   Benz[a]anthracene
24.62 -   Chrysene
28.13 -   Benzo[b]fluoranthene
28.20 -   Benzo[k]fluoranthene
29.13 -   Benzo[a]pyrene
33.29 -   Indeno[1,2,3-cd]pyrene
33.37 -   Dibenz[ah]anthracene
34.41 -   Benzo[ghi]perylene




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