| |
|
|
|
Direct Liquid Chromatographic Separation of Enantiomers on Immobilized Protein Stationary Phases:
VI. Optical Resolution of a Series of Racemic Barbiturates. Studies of Substituent and Mobile Phase Effects
|
|
Method:
|
Matrix
|
Application-No.:
|
|
HPLC
|
-
|
105810
|
|
|
|
| Substances: |
|
benzonal |
| Column: |
|
EC 150/4 RESOLVOSIL® BSA-7 |
| Phase: |
|
Resolvosil BSA-7 |
| MN catalog number: |
|
720046.40 |
|
|
|
| Sample pretreatment: |
|
|
|
|
|
| Conditions: |
|
eluent: 50mM phosphate buffer pH 7.6, 6% 1-propanol
flow rate: 1.0ml/min |
|
|
|
Detection
Subsequent analysis: |
|
UV, 210nm, 0.08 AUFS |
|
|
|
| Author(-s): |
|
Allenmark, S. |
| Source: |
|
J. Chromatogr. 436 (1988) 479 - 483 |
|
|
|
| Keywords: |
|
enantiomers; barbiturates; anticonvulsant |
|
|
|
|
|
|
Chromatogram:
|
|
|
|
|
|
|
| Legend: |
|
Optical resolution of the racemic anticonvulsant benzonal. |
| www.mn-net.com |
 |
Concerning questions to literature applications please contact the cited author/s. Chemicals mentioned in applications are not manufactured or sold by MACHEREY-NAGEL. Applications mentioned in MACHEREY-NAGEL literature or databases are provided for informational purposes only. MACHEREY-NAGEL does not warrant that all applications have been tested in MACHEREY-NAGEL laboratories using MACHEREY-NAGEL products.
MACHEREY-NAGEL does not warrant the correctness of the applications. |
|
 |
|
|