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| Substances: | | naphthalene; acenaphthylene; acenaphthene; fluorene; phenantrene; anthracene; fluoranthene; pyrene; benz[a]anthracene; chrysene; benzo[b]fluoranthene; benzo[k]fluoranthene; benzo[a]pyrene; dibenz[ah]anthracene; benzo[ghi]perylene; indeno[1,2,3-cd]pyrene |
| Column: | | CC 150/4 NUCLEOSIL® 100-5 C18 PAH, 150 x 4 mm ID |
| Phase: | | NUCLEOSIL 100-5 C18 PAH |
| MN catalog number: | | |
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| Sample pretreatment: | | 10 μg/ml each in acetonitrile |
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| Conditions: | | Eluent A: Methanol – water (80:20)
Eluent B: Acetonitrile – tetrahydrofuran (93:7)
Gradient: 0 – 100% B in 10 min, then
5 min at 100% B
Flow rate: 1 ml/min
Pressure: 140 bar
Temperature: 20 °C |
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Detection
Subsequent analysis: | | UV, 260 nm |
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| Author(-s): | | LC department |
| Source: | | MACHEREY-NAGEL |
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| Keywords: | | pah; epa |
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Chromatogram:
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| Legend: | | 1. Naphthalene
2. Acenaphthylene
3. Acenaphthene
4. Fluorene
5. Phenantrene
6. Anthracene
7. Fluoranthene
8. Pyrene
9. Benz[a]anthracene
10. Chrysene
11. Benzo[b]fluoranthene
12. Benzo[k]fluoranthene
13. Benzo[a]pyrene
14. Dibenz[ah]anthracene
15. Benzo[ghi]perylene
16. Indeno[1,2,3-cd]pyrene |