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Separation of PAHs according to EPA 610 on an OPTIMA 5 column.

Method:
Matrix
Application-No.:
GC
-
200510

Substances:naphthalene; acenaphthylene; acenaphthene; fluorene; phenanthrene; anthracene; fluoranthene; pyrene; benzanthracene; chrysene; benzofluoranthene; benzopyrene; indenopyrene; dibenzanthracene; benzoperylene
Column:OPTIMA 5 - 30 m x 0.32 mm ID, 0.25 um Film
Phase:OPTIMA 5
MN catalog number:726314.30
Sample pretreatment:
Conditions:Sample: PAH test mixture according to EPA (20 ug/ml each in toluene)
Injection volume: 1.0 μl
Carrier gas: Hydrogen, 70 KPa
Split: 1 : 15
Temperature: 100 °C, 7 °C/min to 300 °C
Detection
Subsequent analysis:
FID 300 °C, 2^4

Author(-s):Macherey-Nagel
Source:GC department

Keywords:pah; epa 610
Chromatogram:



Legend:Naphthalene
Acenaphthalene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthrene
Pyrene
Benz[a]anthracene
Chrysene
Benzo[b]fluoranthene
Benzo[k]fluoranthene
Benzo[a]pyrene
Indeno[1,2,3-cd]pyrene
Dibenz[ah]anthracene
Benzo[ghi]perylene



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