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Determination of Pesticides in Food Samples (QuEChERS)

Method:
Matrix
Application-No.:
SPE
Fruits, Vegetables
303770

Substances:Pesticides
Column:CHROMABOND Diamino (adsorbent)
Phase:CHROMABOND Diamino
MN catalog number:730653.20
Sample pretreatment:10 g sample are homogenised with 10 mL acetonitrile. After adding the internal standard the sample is shaken with 4 g MgSO4 and 1 g NaCl and centrifuged afterwards. 1 mL of the supernatant is spiked with 25 mg CHROMABOND® Diamino and 150 mg MgSO4 and shaken again.
Conditions:After centrifugation the supernatant is injected into GC MS.
Detection
Subsequent analysis:
Recommended GC-MS

Author(-s):Anastassiadis S.
Source:Journal of AOAC International 2003, 86, No. 2, 412-431 (CVUA Stuttgart), www.QuEChERS.com

Keywords:Pesticides; Fruits; Vegetables; Food; QuEChERS
Chromatogram:


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