| |
|
|
| Separation of EFSA PAHs on NUCLEODUR® C18 PAH |
|
Method:
|
Matrix
|
Application-No.:
|
|
HPLC
|
|
123930
|
|
|
|
| Substances: |
|
benzo[c]fluorene; cyclopenta[cd]pyrene; benz[a]anthracene; chrysene; 5-methylchrysene; benzo[j]fluoranthene; benzo[b]fluoranthene; benzo[k]fluoranthene; benzo[a]pyrene; dibenzo[a,l]pyrene; dibenz[a,h]anthracene; benzo[ghi]perylene; indeno[1,2,3-cd]pyrene; dibenzo[a,e]pyrene; dibenzo[a,i]pyrene; dibenzo[a,h]pyrene |
| Column: |
|
EC 125/4 NUCLEODUR® C18 PAH, 3 µm |
| Phase: |
|
NUCLEODUR® C18 PAH |
| REF number: |
|
760784.40 |
|
|
|
| Sample pretreatment: |
|
EFSA PAH mixture, c=10 mg/l
|
|
|
|
| Conditions: |
|
Eluent A: methanol / water (70:30, v/v)
Eluent B: acetonitrile
Gradient: 0-20 % B in 1.5 min, 20-50 % B in 1.5 min, 50-100 % B in 6 min, 100 % B for 13 min, 100-0 % B in 0.5 min
Flow rate: 1.5 ml/min
Temperature: 35 °C
Injection volume: 2 µl
|
|
|
|
| Detection: |
|
UV, 251 nm |
|
|
|
| Author(-s): |
|
HPLC department
|
| Source: |
|
MACHEREY-NAGEL, Germany 2010 |
|
|
|
| Keywords: |
|
PAHs; EFSA |
|
|
|
|
|
|
Chromatogram:
|
|
|
|
|
|
|
| Legend: |
|
1 - benzo[c]fluorene
2 - cyclopenta[cd]pyrene
3 - benz[a]anthracene
4 - chrysene
5 - 5-methylchrysene
6 - benzo[j]fluoranthene
7 - benzo[b]fluoranthene
8 - benzo[k]fluoranthene
9 - benzo[a]pyrene
10 - dibenzo[a,l]pyrene
11 - dibenz[a,h]anthracene
12 - benzo[ghi]perylene
13 - indeno[1,2,3-cd]pyrene
14 - dibenzo[a,e]pyrene
15 - dibenzo[a,i]pyrene
16 - dibenzo[a,h]pyrene
|
| www.mn-net.com |
 |
Concerning questions to literature applications please contact the cited author/s. Chemicals mentioned in applications are not manufactured or sold by MACHEREY-NAGEL. Applications mentioned in MACHEREY-NAGEL literature or databases are provided for informational purposes only. MACHEREY-NAGEL does not warrant that all applications have been tested in MACHEREY-NAGEL laboratories using MACHEREY-NAGEL products.
MACHEREY-NAGEL does not warrant the correctness of the applications. |
|
 |
|
|